Approximate time required

Solution
1H - 30 min.
13C - 1 hr
31P - 30 min.

Solid state
11B - 30 min.
13C - 1 to 4 hrs
27Al - 30 min.
29Si - 4 to 12 hrs
31P - 30 min.
Please note that solid state 1H NMR high resolution accessory is not available; Hence this work can not be carried out.